Transformer
Oil Gas Analyzer (TOGA) GC System - DISCONTINUED |
10-11
|
|
|
- HID, FID
and/or TCD Detectors
- Built-in
PeakSimple Data System
- Built-in
Standards Preparation ModuleMake Your Own Standards
- Dual 10-port
Gas Sampling Valves
- Gas Extraction
Loop
...on the compact 8610C chassis
|
|
|
By
analyzing the gases dissolved in transformer oil, potential transformer
faults can be avoided. ASTM D3612 provides for identification and
quantification of dissolved gases intransformer oil by GC. The SRI
TOGA GC uses the version referred to as D3612B, the direct injection
technique where the dissolved gas extraction takes place inside the
GC. This means that other than collecting the transformer oil in a
glass airtight syringe, no sample preparation is necessary prior to
injection into the TOGA GC. This helps to avoid contamination made
possible by transferring the sample between various containers. |
The
presence and quantities of certain gases in the transformer oil
indicate four broad types of possible general fault conditions:
|
1-Transformer
oil overheating: methane, ethane, ethylene, and small
quantities of acetylene
2-Partial Discharge: hydrogen, methane, and small
quantities of acetylene and ethane
3-Sustained Arcing: hydrogen, acetylene, and ethylene
4-Insulating Paper Overheating: carbon monoxide
and carbon dioxide
|
|
To achieve
these chromatograms, a transformer oil standard was pumped through the gas
extraction loop of a TOGA GC equipped with HID and TCD detectors. The TCD
was used to quantify the oxygen and nitrogen because the HID is too sensitive
for the large quantities typically found dissolved in transformer oil. |
|
Concentration
by Weight:
Hydrogen 10.7ppb
Oxygen 25.74ppm
Nitrogen 76.65ppm
Methane 70.6ppb
Carbon monoxide 207.4ppb
Carbon dioxide 518ppb
Ethylene 120.9ppb
Ethane 120.7ppb
Acetylene 86.7ppb |
|
In the
TOGA GC, the transformer oil sample is injected by peristaltic pump through
a unique gas extraction loop. The gas extraction loop consists of permeation
membrane tubing encapsulated in a trap-heated glass tube. The permeation
tubing is plumbed to the sample inlet, the dual 10-port valves, and the
waste/sample outlet. Solenoid valves are included for purging the gas extraction
chamber with helium between runs. |
|
While the transformer
oil is being pumped through the gas extraction loop, the 10-port electrically
actuated valves are in the LOAD position. During this time, the dissolved
gases in the transformer oil permeate through the membrane, into the
extraction chamber. When the valves are switched to the INJECT position,
the contents of the loop are swept into the Silica Gel and Molecular
Sieve 13X columns. |
|
|
|
By reconnecting
a few tubing lines, the TOGA GC can be used to create dissolved gas
standards. A Tedlar bag (or other container) filled with gas standard
is connected to the standard pump. The standards preparation vessel
is filled with sample liquid. The standard pump bubbles gas standard
through the standards preparation vessel, equilibrating the liquid
over time to a known concentration. |
|
|
8610-0031
|
TOGA
GC System with HID detector and 1 channel data system |
DISCONTINUED
|
8610-0032
|
TOGA GC System
with TCD & HID detectors and 4 channel data system |
DISCONTINUED
|
(VOLTAGE:
for 110VAC, use "part number-1" [ex: 8610-0032-1] for
220VAC, use "part number-2")
|
|
|
Transformer
Oil Gas Analyzer (TOGA) GC System |
10-11
|
|
|