On-Column
PTV Injector |
60
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- Inject
larger volumes onto narrow bore columns
- Concentrate
sample and focus peaks
- Less bulky
than conventional PTVs
- Simpler
than split/splitless injectors
- Great
for semivolatile samples
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The
On-Column PTV injector is a resistively heated precolumn, which is
connected to your narrow bore column with a special, electrically
insulated split "T" inside the GC column oven. The 5 micron
nonpolar phase in the OCPTV precolumn has a high capacity to absorb
high boiling compounds, and is stable at high temperatures. Like in-tube
SPME, the precolumn discriminates in favor of high boiling semivolatile
analytes, concentrating them in the phase. Like the heated split/splitless
injector, the OCPTV vents the solvent without expanding it to a gas.
Therefore, the OCPTV is capable of larger liquid injections than a
regular heated split/splitless injector. |
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The GC operator injects
sample via syringe through the on-column injection port with the split
vent open to vent the solvent. After injection and solvent venting, the
precolumn heats up while the carrier gas flows through it to sweep focused
analytes from the precolumn to the analytical column. At this point, the
precolumn is hotter than the column oven. The temperature difference between
the hotter precolumn and cooler analytical column causes the analytes
to focus on the analytical column, resulting in sharp peaks on the chromatogram.
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This chromatogram
was generated by an SRI GC equipped with an OCPTV injector and an FID
detector. A 25 meter narrow bore capillary column was used to separate
100ppm diesel range organics (DRO).
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8690-0037
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OCPTV
Injector
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£1,360.00
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On-Column
PTV Injector |
60
|
|
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